HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86747903, compound → HCID 86747902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86747903 | HCID 86747903 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86747902 | HCID 86747902 | — |
Reaction Steps
Mix 2-(N-t-butyloxycarbonylamino)-5-(O-benzyloxy)-3-pentenoic acid, t-butyl ester (2.0 g, 5.3 mmol) and 10% palladium/carbon (0.5 g) in 95% ethanol (40 mL). Hydrogenate at room temperature at atmospheric pressure. Filter and evaporate the filtrate in vacuo to give 2-(N-t-butyloxycarbonylamino)-5-hydroxy-3-pentenoic acid, t-butyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05318992 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-8c6831e643494a269411bcfa39398821 |
| Source note | uspto-grants-1994_06 |