HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178487441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(7-Methoxynaphthalen-1-yl)ethan-1-amine hydrochloride | HCID 16050055 | — |
| Reactant | HCID 178479698 | HCID 178479698 | — |
| Solvent | Chloroform water | HCID 22418719 | — |
| Product | HCID 178487441 | HCID 178487441 | — |
Reaction Steps
0.01 mol of 2-(7-methoxynaphth-1-yl)ethylamine hydrochloride is dissolved in 60 ml of a chloroform/water mixture, and 0.025 mol of potassium carbonate is added under magnetic agitation. The mixture is cooled, and 0.012 mol of 4-imidazoleacetyl chloride hydrochloride is added dropwise. The agitation is maintained for 30 minutes at room temperature and the chloroform phase is evaporated to dryness. The residue is then recrystallized.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05318994 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-96578e6e9a2b46a5883bfca6b9302c16 |
| Source note | uspto-grants-1994_06 |