HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 54344336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 54201704 | HCID 54201704 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54344336 | HCID 54344336 | 60.5% |
Reaction Steps
N-(N-Hydroxycarbamoyl)-3-(3,5-di-tert-butyl-4-hydroxybenzylidene)pyrrolidin-2-one (Ia-4)(2 g, 5.55 mmole), acetic anhydride (680 mg, 6.66 mmole), and pyridine (10 ml) were reacted according to the same method as in Example 22, whereby 1.35 mg of the objective compound (Ia-17) was obtained in 60.5% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05319099 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-7a8a98eed4164547b6d2e1c3d6e93483 |
| Source note | uspto-grants-1994_06 |