HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromopyrrolidin-2-one → HCID 19022166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromopyrrolidin-2-one | HCID 10103471 | — |
| Reactant | HCID 86747910 | HCID 86747910 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19022166 | HCID 19022166 | 63.7% |
Reaction Steps
Substantially in the same manner as in Example 39 (1), 8.2 g (50 mmol) of 3-bromopyrrolidin-2-one and 9.91 g (55 mmol) of N-dimethylaminophenylcarbamate in 100 ml of pyridine were treated to give 7.96 g of the objective compound as white crystal in 63.6% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05319099 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-d87888a323ec452d85354c8b63b7b41e |
| Source note | uspto-grants-1994_06 |