4-Bromobutyronitrile → HCID 22401910, compound

HRID 1109556Notes

Reaction equation

HRID 1109556 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:16]=[CH:17][C:18]=1[Cl:19])[CH2:5][NH:6][CH2:7][C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[C:10]([Cl:15])[CH:9]=1.Br[CH2:21][CH2:22][CH2:23][C:24]#[N:25]>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:16]=[CH:17][C:18]=1[Cl:19])[CH2:5][N:6]([CH2:21][CH2:22][CH2:23][C:24]#[N:25])[CH2:7][C:8]1[CH:13]=[CH:12][C:11]([Cl:14])=[C:10]([Cl:15])[CH:9]=1

Participants

3

Reactant 2

HCID 214124-BromobutyronitrileHCID 4850930HCID 4850930, compound

Product 1

HCID 22401910HCID 22401910, compound

Procedure

Using a procedure analogous to Example 6, Bis-(3,4-dichlorobenzyl)amine (2.71g, 8.09mM) was reacted with 4-bromobutyronitrile (0.81ml) to give the title compound as an oil 1.97g. Ir (film) CN 2230cm-1.

Sources & evidence

ORD record
ord-5954e04b486d4db68a66eb51c4ce55fb
Source dataset
uspto-grants-1994_06
Patent number
US05321047

Reaction notes

Loading…