HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 15229710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | HCID 19020992 | HCID 19020992 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15229710 | HCID 15229710 | 55% |
Reaction Steps
In step 1, 1,3,6,8 tetramethylacridine-9-carboxylic acid was esterified with phenol in THF and 4-dimethylamino-pyridine [DMAP]. Phenyl-1,3,6,8-tetramethylacridine-9-carboxylate was obtained in about 55% yield after recrystallization from benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05321136 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-00e4f7a6c70549a3821305e447111073 |
| Source note | uspto-grants-1994_06 |