HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-formylbenzoate → HCID 19102613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-formylbenzoate | HCID 639145 | — |
| Reactant | Phosphonium, triphenyl(2-pyridinylmethyl)-, chloride | HCID 11058219 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19102613 | HCID 19102613 | 45.4% |
Reaction Steps
Using the procedure of Preparation H1, 750 mg of methyl 3-formylbenzoate, 2.14 g of triphenyl 2-pyridylmethyl phosphonium chloride and 2.0 ml of a 2.5M solution of n-butyl lithium in 30 ml of dry tetrahydrofuran gave 496 mg of the titled product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05322847 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-c6401d457251463eb48286b76f2e344e |
| Source note | uspto-grants-1994_06 |