HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19019919, compound → Dimethyl 4-fluorobenzene-1,2-dicarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19019919 | HCID 19019919 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Dimethyl 4-fluorobenzene-1,2-dicarboxylate | HCID 22744505 | — |
Reaction Steps
Dimethyl 5-bromo-4-fluoro-3,4,5,6-tetrahydrophthalate was dissolved in methylene chloride and stirred over basic alumina for 4 hours. An aliquot was removed and the major product shown to be dimethyl 4-fluorophthalate by GC analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05322954 |
| Source dataset | uspto-grants-1994_06 |
| ORD ID | ord-9bdd53337b27473b95d89571c4b493fc |
| Source note | uspto-grants-1994_06 |