Myristoyl chloride → HCID 53986425, compound

HRID 1110297Notes

Reaction equation

[N+:1]([C:4]1[CH:5]=[C:6]([OH:11])[C:7](=[CH:9][CH:10]=1)[OH:8])([O-:3])=[O:2].[C:12](Cl)(=[O:26])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]>>[O:26]=[C:12]([O:11][C:6]1[CH:5]=[C:4]([N+:1]([O-:3])=[O:2])[CH:10]=[CH:9][C:7]=1[O:8][C:12](=[O:26])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25]

Participants

Reactant 2

HCID 66986Myristoyl chloride

HCID 35051094-Nitrocatechol

Product 1

HCID 53986425HCID 53986425, compound

Procedure

Using this procedure, the reaction of 4-nitrocatechol with tetradecanoyl chloride gave 3,4-bis [(1-oxotetradecyl)oxy]nitrobenzene (mp 58°-60°, Anal. Calcd for C34H57NO6 : C, 70.72; H, 9.98; N, 2.43. Found: C, 70.91; H, 9.61; N, 2.41.

Sources & evidence

ORD record: ord-70f86eb6f3b94081b16aee2e6c36817d
Source dataset: uspto-grants-1994_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05324747

Reaction notes

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