反应详情

N-Acetyl 2,4,5 trimethylthioaniline was prepared by dissolving 2,4,5 trimethylthioaniline (33 g, 0.143 mol) in 200 mL of acetic anhydride at room temperature. Ligroin (800 mL) was added and the mixture was stirred and cooled until the product precipitated. The solid was collected and dried (24 g, 62% yield), mp 87-89° C.

1. temperaturecooled until the product
2. customprecipitated
3. customThe solid was collected
4. customdried (24 g, 62% yield), mp 87-89° C.