HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67922659, compound → HCID 67922774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67922659 | HCID 67922659 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 67922774 | HCID 67922774 | 100% |
Reaction Steps
A mixture of cis-3-methoxy-N,N-dimethyl-1-(phenylmethyl)-4-piperidinamine was hydrogenated at normal pressure and at room temperature with 5 parts of palladium-on-charcoal catalyst 10%. After the calculated amount of hydrogen was taken up, the catalyst was filtered off and the filtrate was evaporated, yielding 17 parts (100%) of cis-3-methoxy-N,N-dimethyl-4-piperidinamine (int. 28).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04975439 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-64e0b8318d90496486c7a911fd07c6b6 |
| Source note | uspto-grants-1990_12 |