HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isopropoxy-4-nitrotoluene → 4-Methyl-2-(propan-2-yloxy)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isopropoxy-4-nitrotoluene | HCID 592731 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Methyl-2-(propan-2-yloxy)aniline | HCID 15068114 | — |
Reaction Steps
5-Methyl-1-(1-methylethoxy)-2-nitrobenzene, 17.7 g (91 mmol), is dissolved in methanol, palladium on charcoal is added and the mixture is exposed to hydrogen gas until the required amount of hydrogen is absorbed. The mixture is worked up in the usual manner to give 15 g of 4-methyl-2-(1-methylethoxy)benzenamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04975456 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-7e4950a4355741209f6cd1b0394f8712 |
| Source note | uspto-grants-1990_12 |