HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 14257862, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Benzeneacetic acid, 4-bromo- | HCID 74654 | — |
| Reactant | Dimethylthexylsilyl chloride | HCID 144239 | — |
| Product | HCID 14257862 | HCID 14257862 | — |
Reaction Steps
This intermediate (hereinafter "intermediate A") was prepared in two steps. 4-Bromophenylacetic acid underwent diborane (B2H6) reduction. A solution of the resulting alcohol then underwent silylation with sodium hydride (NaH) and thexyl dimethyl silyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04975452 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-89e2d1a3c6944de384b7e64bc3f89016 |
| Source note | uspto-grants-1990_12 |