HRID1110483

反应详情

EQUATION

反应方程式

HRID 1110483 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 3.4 g of 4-(4-isoquinolinyl)-3-butyn-1-ol in 35 mL of ethanol was hydrogenated over 0.35 g of 10% Pd/C at room temperature and atmospheric pressure for 5 hours. The catalyst was removed by filtration and the filtrate was evaporated to yield 3.3 g of (E)-4-(4-isoquinolinyl)-3- buten-1-ol as an oil.

WORKUP

后处理

  1. customThe catalyst was removed by filtration
  2. customthe filtrate was evaporated