HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenol → HCID 14347443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenol | HCID 980 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | HCID 14347303 | HCID 14347303 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14347443 | HCID 14347443 | 89.7% |
Reaction Steps
As in Example 115, (2E,4Z)-5-(3-methoxyphenyl)-2,4-nonadienoic acid (7.37 g) and 4-nitrophenol (4.89 g) in 30 mL of dichloromethane was reacted with 1,3-dicyclohexylcarbodiimide (5.91 g). The mixture was stirred at room temperature for 3 days and the usual work up furnished 9.69 g of (2E,4Z)-5-(3-methoxyphenyl)-2,4-nonadienoic acid 4-nitrophenyl ester as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04975438 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-71081207396945b88fe3378d6498c0a6 |
| Source note | uspto-grants-1990_12 |