HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenol → HCID 14547252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenol | HCID 980 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | HCID 14347296 | HCID 14347296 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14547252 | HCID 14547252 | 73.8% |
Reaction Steps
As in Example 115, (E,E)-5-(4-methoxyphenyl)-2,4-tridecadienoic acid (4.75 g) and 4-nitrophenol (2,5 g) in 25 mL of dichloromethane was treated with 1,3-dicyclohexylcarbodiimide (3.1 g) and the mixture was stirred at room temperature for 18 hours. After the usual work up, 4.85 g of (E,E)-5-(4-methoxyphenyl)-2,4-tridecadienoic acid 4-nitrophenyl ester was obtained as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04975438 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-3a5f5ef46da042ac89192e552400489c |
| Source note | uspto-grants-1990_12 |