HRID1110685

反应详情

EQUATION

反应方程式

HRID 1110685 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

According to a known method, optically active 2-octyl bromide and 2,7-dihydroxylfluorenone were reacted in ethanol in the presence of potassium hydroxide. The resultant reaction mixture was purified by a column chromatography and recrystallization to obtain optically active 2-hydroxy-7-(2-octyloxy)-fluorenone.

WORKUP

后处理

  1. customThe resultant reaction mixture
  2. customwas purified by a column chromatography and recrystallization