HRID1110695

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID192414

未命名化合物

结构：CC(C)[C@H](NC(=O)CNC(=O)[C@H](Cc1ccccc1)NC(=O)CNC(=O)OC(C)(C)C)C(=O)NCC(=O)OCc1ccccc1

HCID131715248

未命名化合物

PRODUCTS

生成物

结构：CC(C)[C@H](NC(=O)CNC(=O)[C@H](Cc1ccccc1)NC(=O)CNC(=O)OC(C)(C)C)C(=O)NCC(=O)O

HCID131715252

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID962

Water

H2O

PROCEDURE

实验过程

IV was hydrogenated and worked up as described for VIII to obtain the product in quantitative yield. Rf3 0.16. Anal. calcd. for C25H37N5O8 .H2O: C 54.23, H 7.10, N 12.65%. Found: C 54.14, H 6.93, N 12.21%.

WORKUP

后处理

customto obtain the product in quantitative yield

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-ab9bc33211ea4e7ca00c7c8c09eab75b
来源数据集: uspto-grants-1990_12
DOI: 10.6084/m9.figshare.5104873.v1
专利: US04976734
来源说明: uspto-grants-1990_12

反应 SMILES

[NH:1]([C:39]([O:41][C:42]([CH3:45])([CH3:44])[CH3:43])=[O:40])[CH2:2][C:3]([NH:5][C@H:6]([C:14]([NH:16][CH2:17][C:18]([NH:20][C@H:21]([C:25]([NH:27][CH2:28][C:29]([O:31]CC1C=CC=CC=1)=[O:30])=[O:26])[CH:22]([CH3:24])[CH3:23])=[O:19])=[O:15])[CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:4].N(C(OC(C)(C)C)=O)[C@H](C(NCC(O)=O)=O)C>O>[NH:1]([C:39]([O:41][C:42]([CH3:44])([CH3:43])[CH3:45])=[O:40])[CH2:2][C:3]([NH:5][C@H:6]([C:14]([NH:16][CH2:17][C:18]([NH:20][C@H:21]([C:25]([NH:27][CH2:28][C:29]([OH:31])=[O:30])=[O:26])[CH:22]([CH3:24])[CH3:23])=[O:19])=[O:15])[CH2:7][C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)=[O:4]