反应详情

N-(3-Fluorophenyl)aniline (7.02 g, 0.0375 mole) and chloroacetyl chloride (3.3 ml, 0.0412 mole) were refluxed in benzene (50 ml) for 3 hours, then evaporated in vacuo to solids and the solids triturated with pentane and ether to yield purified title product, 8.69 g, m.p. 115°-117°.

1. customevaporated in vacuo to solids
2. customthe solids triturated with pentane and ether
3. customto yield
4. custompurified title product, 8.69 g, m.p. 115°-117°