HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → Anthraquinone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | 1-Amino-4-bromo-9,10-dihydro-9,10-dioxo-2-anthracenesulfonic acid | HCID 22628 | — |
| Edukt | 4-(beta-Acetylaminoethylamino)aniline 3-sulfonic acid | HCID 22154633 | — |
| Produkt | Anthraquinone | HCID 6780 | — |
Reaktionsschritte
1-Amino-4-bromoanthraquinone-2-sulfonic acid and 4-(β-acetylaminoethylamino)aniline-3-sulfonic acid were subjected to Ullmann condensation in the presence of cuprous chloride as a catalyst, followed by hydrolysis of the acetyl group under an acid condition of hydrochloric acid, thereby obtaining an anthraquinone intermediate compound of the following formula (2) in the free acid form. ##STR244##
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04977261 |
| Quelldatensatz | uspto-grants-1990_12 |
| ORD ID | ord-dfdc822a61ad45f98c39faa65df17554 |
| Quellennotiz | uspto-grants-1990_12 |