HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14478725, compound → HCID 14478727, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14478725 | HCID 14478725 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14478727 | HCID 14478727 | 96% |
Reaction Steps
The resultant compound from Example 8 (107 mg, 0.313 mmol) and 10% palladium on carbon (110 mg) in methanol (10 mL) were stirred under a hydrogen atmosphere for 18 hours. The mixture was filtered and evaporated to afford 94.6 mg (96%) of the desired compound, Mass spectrum: (M+H)+ =317.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04977277 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-6a1e34a883e0418b99b3ca87829e08c2 |
| Source note | uspto-grants-1990_12 |