Hydrochloric Acid → HCID 15631263, compound

Participants

Reaction Steps

The resultant compound from Example 55 (114 mg, 0.355 mmol) in dioxane (4 ml) and water (2 ml) at 0° C. was treated with LiOH monohydrate (42.0 mg, 1 mmol). After 90 min 2M HCl (0.6 ml, 1.2 mmol) was added and the mixture was evaporated to a foam which was used without further purification, DCI-MS: (M+H)=327.

Provenance & Evidence