HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 86744424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 22153300 | HCID 22153300 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 86744424 | HCID 86744424 | — |
Reaction Steps
A stirred solution of 104.7 g (0.3 mole) of 2-(4-bromomethylphenyl)-5-nitrobenzthiazole and 78.6 g (0.3 mole) of triphenylphosphine in xylene is heated at reflux for 19 hours. Compound B then is isolated by filtration, washed with additional portions of xylene, and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978476 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-071f6fbb72d44cc98b82b0e62328d283 |
| Source note | uspto-grants-1990_12 |