HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 86744428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 22153306 | HCID 22153306 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 86744428 | HCID 86744428 | — |
Reaction Steps
A stirred solution of 90.4 g (0.3 mole) of 1-methyl-2-(4-bromomethylphenyl)benzimidazole and 78.7 g (0.3 mole) of triphenylphosphine in xylene is heated at reflux for 19 hours. Compound B is then isolated by filtration, washed with additional portions of xylene, and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978476 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-b826c7e25fac4d9c85230243b4cd834b |
| Source note | uspto-grants-1990_12 |