HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → Cyclohexaneacetaldehyde, alpha-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Product | Cyclohexaneacetaldehyde, alpha-methyl- | HCID 95560 | — |
Reaction Steps
100.0 g of a compound (Ia) was hydrogenated in a solution of 2 g of p-toluene sulfonic acid, 200 ml of acetone, and 500 ml of water at 60° C. for 24 hours. The hydrogenated product was distilled to obtain 66.5 g of 2-cyclohexylpropanal (purity: 98.5%, boiling point: 65° C./5 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978653 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-00699f0702244611a5fc978506e295cc |
| Source note | uspto-grants-1990_12 |