HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19807226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Glyoxylic Acid | HCID 760 | — |
| Reactant | 7-Methyltryptamine | HCID 26714 | — |
| Product | HCID 19807226 | HCID 19807226 | — |
Reaction Steps
7-Methyltryptamine (free base, Sigma) was dissolved in aqueous hydrochloric acid and condensed with glyoxylic acid as described in part B. The product was decarboxylated according to part C to yield 8-methyl-1,2,3,4-tetrahydro-beta-carboline hydrochloride, which was recrystallized from ethanol:water R1-7 =R9 =H; R8 =Me).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978669 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-0c66309870014f0cb7ccac5a7ac4d146 |
| Source note | uspto-grants-1990_12 |