HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetylpyridine → 1-[[[[1-(2-Pyridinyl)ethylidene]hydrazino]carbonyl]methyl]pyridinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetylpyridine | HCID 14286 | — |
| Reactant | Pyridinioacetohydrazide chloride | HCID 70773 | — |
| Product | 1-[[[[1-(2-Pyridinyl)ethylidene]hydrazino]carbonyl]methyl]pyridinium chloride | HCID 73867310 | — |
Reaction Steps
Following the general method of Example 2 and making non-critical variations, 5.63 gm (0.03 mole) of Girard's Reagent P and 3.63 gm (0.03 mole) of 2-acetylpyridine yield 5.70 gm (65%) of the title compound; mp 183.7° (decomp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978670 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-1a59fc28191c46358605d52e488870da |
| Source note | uspto-grants-1990_12 |