Allyl bromide → HCID 86744382, compound

Participants

Reaction Steps

Into a 500 ml flask fitted with a reflux condenser and a heating mantle was placed tris(3,6-dioxaheptyl)amine (14.55 g, 45 mmoles) and 150 ml acetone. Allyl bromide (6.53 g, 54 mmoles, 20% excess) was added and the solution brought to reflux. After 28 hours the 1H-NMR spectrum indicated that the starting amine had been consumed. Removal of the solvent in vacuo gave crude product, N-(2-propeny)-N,N,N-tris(3,6-dioxaheptyl)ammonium bromide, as an amber oil (yield 19.66 g, 98%).

Provenance & Evidence