HCID 15137045, compound → HCID 15137046, compound

Participants

Reaction Steps

A solution of 0.125 g (0.59 mmol) of the product of Example 5, Step C and 50 mg of 5% Pd/C in 10 mL of ethyl acetate was shaken under 40 psi H2 for 1 h. The solution was filtered through Celite and the filtrate concentrated to a colorless oil that crystallized from ethyl acetate-hexane to afford 0.120 g (98%) of white prisms.

Provenance & Evidence