HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vinyl Acetate → 1,1-Ethanediol, 1,1-diacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vinyl Acetate | HCID 7904 | — |
| Catalyst | Palladium Chloride | HCID 24290 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 1,1-Ethanediol, 1,1-diacetate | HCID 222536 | 2,504.6% |
Reaction Steps
The procedure of Example 9 was repeated except that 0.451 g of palladium chloride was used in place of palladium supported on activated carbon and the reaction was effected for 3 hours. GC analysis showed that 1.51 g of vinyl acetate and 32.1 g of ethylidene diacetate were formed with considerable amount of acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978778 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-a9b5c18e35584c908a6278b712e5c952 |
| Source note | uspto-grants-1990_12 |