HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → 3-Aminobenzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | 3-Nitrobenzaldehyde | HCID 7449 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Product | 3-Aminobenzylamine | HCID 4628831 | 88% |
Reaction Steps
Reaction was carried out as in Example 3 except that p-nitrobenzaldehyde was replaced by m-nitrobenzaldehyde. Reaction was complete in 55 minutes, during which hydrogen (15.8 Nl) was absorbed. Successively, post-treatment as in Example 3 was carried out to obtain m-aminobenzylamine having a purity of 99.94% (2.5 g, yield 88.0%, b.p. 131°-132° C./6 mm Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04978792 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-a7a9f0114cc4444bb9db6c312fdafb2d |
| Source note | uspto-grants-1990_12 |