HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 54322291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Ethylparaben | HCID 8434 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 86744435 | HCID 86744435 | — |
| Product | HCID 54322291 | HCID 54322291 | — |
Reaction Steps
1.0 g (0.021 mol) of 50% sodium hydride, 25 ml of dimethylformamide, 3.2 g (0.019 mol) of ethyl 4-hydroxybenzoate and 6.1 g (0.019 mol) of (S)-2-tetrahydropyranyloxypropoxy p-toluenesulfonate were reacted at 60° C. for 8 h. Then the same procedure as in Referential Example 1 was repeated to obtain 5.0 g of the crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04980082 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-168e6b4d379a4f40b31afe2b30e0108e |
| Source note | uspto-grants-1990_12 |