HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 53725720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 54322291 | HCID 54322291 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53725720 | HCID 53725720 | 891.8% |
Reaction Steps
A mixture of 4.5 g (0.014 mol) of (S)-ethyl 4-(2-tetrahydropyranyloxy)propoxybenzoate, 0.2 g (0.0011 mol) of p-toluenesulfonic acid monohydrate and 45 ml of methanol were refluxed for 1 h. Then the same procedure as in Referential Example 2 was repeated to obtain 2.2 g of the crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04980082 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-a1d75bb06e3b487482a6874e6b76a9e2 |
| Source note | uspto-grants-1990_12 |