Gamma-Aminobutyric Acid → HCID 15599255, compound

HRID 1111346Notes

Reaction equation

HRID 1111346 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][C:5]([OH:7])=[O:6].[C:8]1([C:13]([C:15]2[CH:20]=[CH:19][C:18]([S:21](Cl)(=[O:23])=[O:22])=[CH:17][CH:16]=2)=[O:14])[S:12][CH:11]=[CH:10][CH:9]=1>[OH-].[Na+].C(OCC)C>[C:8]1([C:13]([C:15]2[CH:20]=[CH:19][C:18]([S:21]([NH:1][CH2:2][CH2:3][CH2:4][C:5]([OH:7])=[O:6])(=[O:23])=[O:22])=[CH:17][CH:16]=2)=[O:14])[S:12][CH:11]=[CH:10][CH:9]=1

Participants

5

Reactant 2

HCID 119Gamma-Aminobutyric AcidHCID 15599254HCID 15599254, compound

Product 1

HCID 15599255HCID 15599255, compound

Reagents, catalysts & solvents 2

HCID 3283Diethyl EtherSolventHCID 14798Sodium HydroxideSolvent

Procedure

103 mg (1.10-3 mole) of 4-aminobutyric acid dissolved in 4 ml of a 0.5 N solution of caustic soda are added dropwise to 287 mg (1.10-3 mole) of 4-(2-thenoyl)benzenesulphonyl chloride in 5 ml of ethyl ether.

Sources & evidence

ORD record
ord-c387caeec9b04825b1af299d276d758d
Source dataset
uspto-grants-1990_12
Patent number
US04980349

Reaction notes

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