HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22152218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Undecanoic acid, 11-(((4-chloro-2-(2-chlorobenzoyl)phenyl)sulfonyl)amino)- | HCID 3086746 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 22152218 | HCID 22152218 | — |
Reaction Steps
19 g of redistilled thionyl chloride are added to 10.3 g of 11-[2-(2-chlorobenzoyl)-4-chlorobenzenesulphonamido]undecanoic acid in 130 ml of anhydrous benzene. After refluxing for 2 hours, the reaction medium is evaporated to dryness under vacuum and it gives a colourless oil which is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04980349 |
| Source dataset | uspto-grants-1990_12 |
| ORD ID | ord-d9f73d6f765746dc81d2399f97ce08d3 |
| Source note | uspto-grants-1990_12 |