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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1111376Generated: October 29, 2026

Potassium Carbonate → HCID 19826066, compound

https://huagongshe.com/reaction/1111376

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantPhenethylamine, p-fluoro-, hydrochlorideHCID 197725—
ReactantHCID 14837050HCID 14837050—
SolventDimethylformamideHCID 6228—
ProductHCID 19826066HCID 19826066—

Reaction Steps

To 100 ml of dry DMF were added 2-(4-fluorophenyl)ethylamine hydrochloride (10 g) and milled K2CO3 (20 g). After five minutes of stirring, 3-(3-chloropropyl)-5,6-dimethoxy-1,2-benzisoxazole (6.4 g) and KI (0.01 g) were added.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04980365
Source datasetuspto-grants-1990_12
ORD IDord-bb9726dea86d46d2a30450f4e354d04f
Source noteuspto-grants-1990_12