HCID 19753326, compound → HCID 178443240, compound

HRID 1111473Notes

Reaction equation

HRID 1111473 reaction equation
OC1C(=O)C2C(C(=O)C=1)=CC=CC=2.[CH2:14]([NH:18][CH:19]([C:31]1[C:32](=[O:43])[C:33]2[C:38]([C:39](=[O:42])[C:40]=1[OH:41])=[CH:37][CH:36]=[CH:35][CH:34]=2)[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])CCC.C(NC(C1C(=O)C2C(C(=O)C=1)=CC=CC=2)CCCCCCCCCCC)CCC>>[CH3:14][NH:18][CH:19]([C:31]1[C:32](=[O:43])[C:33]2[C:38]([C:39](=[O:42])[C:40]=1[OH:41])=[CH:37][CH:36]=[CH:35][CH:34]=2)[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]

Participants

4

Reactant 3

HCID 19753326HCID 19753326, compoundHCID 178443242HCID 178443242, compoundHCID 178516607HCID 178516607, compound

Product 1

HCID 178443240HCID 178443240, compound

Procedure

The yield relative to 2-hydroxy-1,4-naphthoquinone used for the preparation of 2-(1 butylaminododecyl)-3-hydroxy-1,4-naphthoquinone, was 80.1 mol%. Further, the yield relative to the starting material 2-(1-butylaminododecyl)-1,4-naphthoquinone, was 81.7 mmol%.

Sources & evidence

ORD record
ord-9eda663651484dd09a500fd1dd4683e1
Source dataset
uspto-grants-1990_12
Patent number
US04980489

Reaction notes

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