Sulfuric Acid → HCID 86744447, compound

Participants

Reaction Steps

To a solution, stirred at ambient temperature, of 2.5 g of methyl 4-[(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl) hydroxymethyl] phenylsulfone, obtained in Example I, in 100 cm3 of acetone, there is slowly added the Jones reagent prepared previously by adding 1.9 cm3 of concentrated sulfuric acid to a solution of 2.2 g of potassium bichromate dissolved in 15 cm3 of water. At the end of the addition, the mixture is again stirred for two hours, then left overnight at ambient temperature.

Provenance & Evidence