HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19096124, compound → 4-Phenoxy-3-sulfamoylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19096124 | HCID 19096124 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 4-Phenoxy-3-sulfamoylbenzoic acid | HCID 20334527 | — |
Reaction Steps
6.2 g of 3-N-(3-azabicyclo-[3.2.0]-heptano)-4-phenoxy-5-sulphamylbenzoic acid methyl ester are suspended in 60 ml of 1 N NaOH and the suspension is heated on the waterbath until a clear solution is formed. The acid is then precipitated with 2 N HCl, while stirring well, and is recrystallised from glacial acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04118397 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-def81418fcdf410489442e088eb92d9a |
| Source note | uspto-grants-1978_10 |