HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dinitroaniline → 1,3,5-Triaminobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dinitroaniline | HCID 12068 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 1,3,5-Triaminobenzene | HCID 66952 | 99.6% |
Reaction Steps
A mixture of 1.0 g of 3,5-dinitroaniline, 0.5 g of 10% palladium on carbon catalyst and 100 ml of ethyl acetate is hydrogenated in a Parr shaker, filtered and evaporated to give 670 mg of 1,3,5-benzenetriamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04118418 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-d6b7951141f54d95aec517323e3223de |
| Source note | uspto-grants-1978_10 |