HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 20372149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | N-[1-(Methoxymethyl)-3-(1-naphthyloxy)propyl]-N-methylformamide | HCID 22754995 | — |
| Product | HCID 20372149 | HCID 20372149 | — |
Reaction Steps
N-[1-(Methoxymethyl)-3-(1-naphthyloxy)propyl]-N-methylformamide, described in Example 8, is reduced with LiAlH4 in the manner described in Example 4 to give the title compound, nmr (CDCl3) δ 2.05 (m, 2H), 2.35 (s, 6H), 3.0 (s, 1H), 3.35 (s, 3H), 3.5 (m, 2H), 4.25 (t, J = 5.5Hz, 2H) and 6.75-8.4 (7H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04118511 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-046097c935d84ac7b069b040fa0778ff |
| Source note | uspto-grants-1978_10 |