Ethylamine → HCID 54252219, compound

HRID 1111724Notes

Reaction equation

HRID 1111724 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[C:12](=[CH:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH2:11][CH2:10][CH2:9][C:8]=1[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1.[CH2:26]([NH2:28])[CH3:27]>C1(C)C=CC=CC=1>[CH2:26]([NH:28][CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[C:12](=[CH:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH2:11][CH2:10][CH2:9][C:8]=1[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[CH3:27]

Participants

4

Reactant 2

HCID 6341EthylamineHCID 54203858HCID 54203858, compound

Product 1

HCID 54252219HCID 54252219, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

1-Bromo-4-[[2-phenyl-6-(phenylmethylene)-1-cyclohexen-1-yl]oxy]butane is dissolved in toluene, treated with two equivalents of ethyl amine and allowed to stand at room temperature for 1 day, and washed with potassium carbonate solution. Evaporation of the toluene yields the title compound.

Workup

  1. washwashed with potassium carbonate solution
  2. customEvaporation of the toluene

Sources & evidence

ORD record
ord-860b3c67a2b345b3b0bf92128f720bc7
Source dataset
uspto-grants-1978_10
Patent number
US04118558

Reaction notes

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