HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → tert-Butyl 3,4-dinitrobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | tert-Butanol | HCID 6386 | — |
| Reactant | 3,4-dinitrobenzoyl Chloride | HCID 11806491 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | tert-Butyl 3,4-dinitrobenzoate | HCID 20551560 | 49% |
Reaction Steps
The crude 3,4-dinitrobenzoyl chloride, 500 ml. of benzene, 25 ml. of pyridine and 22 g. (0.3 mole) of t-butyl alcohol were reacted as in Example 2 (A), second paragraph, to provide 33 g. (49 percent yield) of t-butyl 3,4-dinitrobenzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04118573 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-b8e634f05b964b469bb73637f0356efc |
| Source note | uspto-grants-1978_10 |