HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl 2-(4-chlorophenoxy)-2-methylpropionate → HCID 54150661, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl 2-(4-chlorophenoxy)-2-methylpropionate | HCID 104099 | — |
| Reactant | Sodium Salicylate | HCID 16760658 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54150661 | HCID 54150661 | — |
Reaction Steps
50 g (0.18 mole) of 1-(2-p-chlorophenoxy-2-methylpropionyloxy)-2-chloro-ethane are mixed with 43.3 g (0.27 mole) of sodium salicylate. The mixture is heated to 195° for 8 hours. The products are taken up in ether, and NaCl is removed by filtration. The diester crystallizes quantitatively from the ether solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04118583 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-ab410b889f8f4719bd568fc7d51c15a8 |
| Source note | uspto-grants-1978_10 |