Methanimidamide, N,N'-bis(3,5-dichlorophenyl)- → HCID 70626931, compound

HRID 1111884Notes

Reaction equation

HRID 1111884 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([NH:9][CH:10]=[N:11][C:12]2[CH:17]=[C:16]([Cl:18])[CH:15]=[C:14]([Cl:19])[CH:13]=2)[CH:5]=[C:6]([Cl:8])[CH:7]=1>CCOCC>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([NH:9][CH:10]=[N:11][C:12]2[CH:17]=[C:16]([Cl:18])[CH:15]=[C:14]([Cl:19])[CH:13]=2)[CH:5]=[C:6]([Cl:8])[CH:7]=1

Participants

3

Reactant 1

HCID 2804832Methanimidamide, N,N'-bis(3,5-dichlorophenyl)-

Product 1

HCID 70626931HCID 70626931, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

N,N'-Bis[3,5-dichlorophenyl]formamidine (2 g.) is dissolved in ether (50 ml) and anhydrous hydrochloric acid is bubbled through the reaction mixture to give 1.9 g. of product, which precipitated from the reaction mixture, m.p. 265°-8° C.

Workup

  1. customanhydrous hydrochloric acid is bubbled through the reaction mixture
  2. customto give 1.9 g
  3. customof product, which precipitated from the reaction mixture, m.p. 265°-8° C.

Sources & evidence

ORD record
ord-c8f4ba28c3784d0fa115f64bed238ca2
Source dataset
uspto-grants-1978_10
Patent number
US04119667

Reaction notes

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