Hexamethylenediamine → HCID 21332364, compound

Participants

Reaction Steps

In a manner similar to that of Example 1, condensation of 1-heptene oxide (71.8 g.) and hexamethylenediamine (32 g.) and recrystallization of the resulting product from ethanol gave N,N'-(1,6-hexylene)-bis[2-hydroxyheptylamine] (I: R = CH3 (CH2)4, R' = H, X = (CH2)6, Z = H)(16.5 g., m.p. 131.2°-134.2° C.).

Provenance & Evidence