HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → N,N'-(1,6-hexylene)-bis[2-hydroxynonylamine]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | N,N'-(1,6-hexylene)-bis[N-methyl-2-hydroxynonylamine] | HCID 21332463 | — |
| Product | N,N'-(1,6-hexylene)-bis[2-hydroxynonylamine] | HCID 21332345 | — |
Reaction Steps
In a manner similar to that of Example 22, methylation of N,N'-(1,6-hexylene)-bis[2-hydroxynonylamine] (36 g.) and treatment of the resulting product (25 g., b.p. 172°-176° C./0.05 mm.) with hydrogen bromide gave N,N'-(1,6-hexylene)-bis[N-methyl-2-hydroxynonylamine] (I: R = CH3 (CH2)6, R' = CH3, X = (CH2)6, Z = H) dihydrobromide (26.3 g., m.p. 176.0°-177.0° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04119668 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-402490edfa454f078f41c35a472da98a |
| Source note | uspto-grants-1978_10 |