HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediamine → HCID 21332393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediamine | HCID 428 | — |
| Reactant | 1,2-Epoxydecane | HCID 16993 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21332393 | HCID 21332393 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-decene oxide (58 g.) and 1,3-propanediamine (13.8 g.) and three recrystallizations of the resulting product from methanol gave N,N'-(1,3-propylene)-bis[2-hydroxydecylamine] (I: R = CH3 (CH2)7, R' = H, X = (CH2)3, Z = H) (8.5 g., m.p. 104.0°-107.6° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04119668 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-8589b141200948338985e1a37fb044b4 |
| Source note | uspto-grants-1978_10 |