HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Octanediamine → HCID 21332399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Octanediamine | HCID 24250 | — |
| Reactant | 2-Pentyloxirane | HCID 92215 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21332399 | HCID 21332399 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-heptene oxide (52 g.) and 1,8-octanediamine (32.8 g.) and two recrystallizations of the resulting product from methanol gave N,N'-(1,8-octylene)-bis[2-hydroxyheptylamine] (I: R = CH3 (CH2)4, R' = H, X = (CH2)8, Z = H) (17.2 g., m.p. 128.0°-132.8° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04119668 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-b23fdcc3420245c2bc5be8bfc11a8953 |
| Source note | uspto-grants-1978_10 |