HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,10-Decanediamine → N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,10-Decanediamine | HCID 1317 | — |
| Reactant | 2-Butyloxirane | HCID 15036 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine] | HCID 21332454 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-hexene oxide (34.8 g.) and 1,10-decanediamine (30 g.) and recrystallization of the resulting product from isopropyl alcohol gave N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine] (I: R = CH3 (CH2)3, R' = H, X = (CH2)10, Z = H) (8.9 g., m.p. 127.0°-137.0° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04119668 |
| Source dataset | uspto-grants-1978_10 |
| ORD ID | ord-89b84062e24a476d9bc8cee62c315568 |
| Source note | uspto-grants-1978_10 |